Información adicional sobre el 3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate
Esta impureza | 3-{2-[(2-metil-5-{[3-(4-metil-1H-imidazol-1-yl)-5-(trifluorometil)fenil]carbamoyl}fenil)(nitroso)amino]pirimidin-4-yl}piridin-1-ium-1-olato | presenta un perfil estructural complejo que incluye grupos nitroso | carbamoilo | anillos imidazol y arilos trifluorometilados y una unidad piridinio-olato que confiere carácter iónico parcial. Su elevada masa molecular y heteroatomía afectan la retención en HPLC y la ionización en LC-MS | mientras que la presencia del grupo nitroso indica un origen por oxidación de aminas precursoras. Especificar controles analíticos es crítico: métodos LC-MS cualitativos y cuantitativos optimizados | validación de extracción y condiciones redox durante síntesis y purificación para minimizar su formación y cumplir requisitos de calidad.
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![3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate](https://veeprho.com/wp-content/uploads/2024/11/VE0022222-3-2-2-methyl-5-3-4-methyl-1H-imidazol-1-yl-5-trifluoromethyl-phenyl-carbamoyl-phenyl-nitroso-amino-pyrimidin-4-yl-pyridin-1-ium-1-olate-sqr.png "3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate")
![3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate](https://veeprho.com/wp-content/uploads/2026/02/Nilotinib-Hydrochloride-Monohydrate-Working-Standard-Secondary-Reference-Standard-923288-90-8-VE0027614.png "3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate")
![3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate](https://veeprho.com/wp-content/uploads/2022/07/Nilotinib-EP-Impurity-B.png "3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate")
![3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate](https://veeprho.com/wp-content/uploads/2022/07/Nilotinib-EP-Impurity-C.png "3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate")
