Apixaban Related Compound 4 (Apixaban Impurity 74) | identificado como 5-clorohexanoil cloruro y registrado bajo CAS 99585-01-0 | es una impureza reactiva presente en procesos de síntesis de apixaban. Como cloruro de acilo alifático exhibe alta reactividad frente a nucleófilos y tendencia a hidrólisis | por lo que requiere manejo anhidro y control de humedad. Su monitoreo analítico se realiza mediante HPLC con detección UV | GC-MS y espectroscopía NMR para confirmación estructural y cuantificación en límites de impureza. Se recomienda establecer parámetros de especificación | condiciones de almacenamiento a baja temperatura y procedimientos de eliminación para garantizar la calidad del API.
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