Diclofenac glyoxilic acid é uma impureza conhecida no processo de fabricação de diclofenaco | correspondendo ao análogo ceto formado por oxidação parcial ou via rota de síntese incompleta. Tecnicamente | apresenta desafios analíticos por sua semelhança estrutural com o princípio ativo | exigindo métodos robustos de separação como HPLC com detector UV | LC MS e confirmação por RMN para identificação inequívoca. Seu acompanhamento é crítico para controle de qualidade e estabilidade | pois pode afetar o perfil de pureza e requisitos de especificação. Estratégias de controle incluem otimização das condições de reação | purificação por cromatografia e validação analítica para limites aceitáveis.
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