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Home / Catalog / Synthesis Attempts and Failure Report / N-Nitroso N-Desmethyl Rifampicin; Synthesis Attempts and Failure Report (NAP Test)
N-Nitroso N-Desmethyl Rifampicin; Synthesis Attempts and Failure Report (NAP Test)
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Dokumentation

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Enthält: HPLC, MASS/LC-MS, 1H-NMR, FT-IR, Gehalt, Structure Elucidation Report (SER) sowie zusätzliche analytische Daten je nach Produkt.

N-Nitroso N-Desmethyl Rifampicin; Synthesis Attempts and Failure Report (NAP Test)

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1 Digital Report (PDF) $4,697.80
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SMILES

O=NN1CCN(/N=C/C2=C(N3)C(O)=C(C(O)=C(C)C(O[C@]4(C)O/C=C/[C@H](OC)[C@@H](C)[C@@]([H])(OC(C)=O)[C@H](C)[C@H](O)[C@H](C)[C@@H](O)[C@@H](C)/C=C/C=C(C)\C3=O)=C5C4=O)C5=C2O)CC1

Experiments

10 synthesis attempts (5 experiments performed twice) under recommended conditions for nitroso impurity formation. Along with HPLC, MASS/LCMS, NMR, IR performed for all 10 synthesis attempts

Report Format

Delivered in digital PDF format. Printed copies available on request (additional shipping and handling charges apply).

Report Language

English by default. Certified translations available at extra cost via our third-party translation partner.

Beschreibung

N-Nitroso N-Desmethyl Rifampicin ist eine vorgeschlagene Nitrosamin-Verunreinigung im Zusammenhang mit N-Desmethyl-Rifampicin, einem Rifampicin-bezogenen Metaboliten bzw. einer verwandten Substanz aus der Rifamycin-Antibiotika-Chemie. Die Verunreinigung wird als mögliches Nitrosierungsprodukt einer nitrosierbaren sekundären Amin- oder verwandten stickstoffhaltigen Struktur betrachtet, die in Gegenwart nitrosierender Reagenzien (z. B. Nitrit/salpetrige Säure) unter sauren Bedingungen das entsprechende N-Nitroso-Derivat bilden könnte.

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