La impureza Valsartan Desvaleryl Cyano (sal HCl) es un derivado relacionado que puede generarse durante etapas de síntesis o por degradación del principio activo | caracterizado por pérdida de la cadena valeril y presencia del grupo ciano en forma de sal clorhidrato. Su identificación y cuantificación son críticas para el control de calidad; se caracteriza mediante HPLC con detección UV | LC-MS y corroboración por RMN para establecer perfil espectral y tiempo de retención. Esta impureza puede afectar pureza y rendimiento de lote | por lo que se establecen límites especificados | estrategias de mitigación como etapas adicionales de purificación | control de pH en reacción y monitoreo en estabilidad.
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