QNMR, D2O Exchange, 13C NMR, 13C APT, COSY NMR, NOESY NMR, 15N NMR, HSQC NMR, HMQC NMR, and HMBC NMR. These are available upon request and may be free or subject to additional charges.
Descrição
Impureza Bicalutamide Oxirane (CAS 90357-51-0) | também conhecida como 2-methyloxirane-2-carboxylic acid N-(4-cyano-3-trifluoromethylphenyl)amide | caracteriza-se por um anel oxirano altamente reativo gerado como subproduto durante etapas de oxidação ou epoxidação na síntese do bicalutamida. De polaridade moderada a elevada | tende a sofrer abertura de anel por hidrólise sob condições ácidas ou básicas. A identificação e quantificação requerem técnicas analíticas de alta resolução como HPLC-DAD e LC-MS com confirmação por RMN 1H/13C. Recomenda-se estabelecimento de limites de especificação | desenvolvimento de métodos de purificação e referência de padrão para controle de qualidade e perfil de impurezas.
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