Impureza de Citalopram 27 (sal de cloreto) é um subproduto identificado no perfil de impurezas do processo de síntese do citalopram | caracterizado por alteração estrutural que pode surgir por reações secundárias durante halogenação ou quaternização. Como sal de cloreto | apresenta maior polaridade e requisitos específicos de controle analítico. A sua identificação e quantificação são realizadas por HPLC acoplada a detectores UV e LC-MS para confirmação de massa | complementadas por RMN para elucidação estrutural. Monitorização de processo | otimização de parâmetros de reação e etapas de purificação são essenciais para conformidade com limites de impurezas ICH e garantia de qualidade do material ativo.
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