QNMR, D2O Exchange, 13C NMR, 13C APT, COSY NMR, NOESY NMR, 15N NMR, HSQC NMR, HMQC NMR, and HMBC NMR. These are available upon request and may be free or subject to additional charges.
Descripción
Impureza de bicalutamida oxirano (Bicalutamide Oxirane Impurity) | CAS 90357-51-0 | 2-Methyloxirane-2-carboxylic acid N-(4-Cyano-3-trifluoromethylphenyl)amide | es un subproducto epóxido observado durante la síntesis y degradación de bicalutamida. Su presencia en el API puede alterar el perfil de pureza y la estabilidad | por lo que su identificación y cuantificación son críticas para control de calidad. Requiere técnicas analíticas sensibles como HPLC-UV acoplado a LC-MS para confirmación estructural y NMR para elucidación | además de métodos validados para cuantificación. El control del proceso | optimización de condiciones de reacción y almacenamiento minimizan su formación y garantizan conformidad con límites basados en guías ICH.
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