QNMR, D2O Exchange, 13C NMR, 13C APT, COSY NMR, NOESY NMR, 15N NMR, HSQC NMR, HMQC NMR, and HMBC NMR. These are available upon request and may be free or subject to additional charges.
설명
Nilotinib EP Impurity B, 즉 Nilotinib Related Compound B는 CAS 18595-18-1, 분자식 C9H11NO2, 분자량 165.19 g/mol의 저분자 방향족 아미노알코올에 해당한다. 그 구조는 니트로사민 계열 불순물이 아니라, 치환된 벤질아민 골격 형성과 연관된 합성 중간체 또는 공정 유래 부산물과 부합한다. 평가는 일반적으로 LC-MS/MS, 고분해능 MS, NMR에 의한 상호보완적 동정이 필요하며, 휘발성이 확보될 경우 유도체화 후 GC-MS도 활용된다. 규제 관점에서 이 성분은 impurity profiling 체계에서 지정된 관련물질로 관리된다.
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![3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate](https://veeprho.com/wp-content/uploads/2024/11/VE0022222-3-2-2-methyl-5-3-4-methyl-1H-imidazol-1-yl-5-trifluoromethyl-phenyl-carbamoyl-phenyl-nitroso-amino-pyrimidin-4-yl-pyridin-1-ium-1-olate.png "3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate")
