QNMR, D2O Exchange, 13C NMR, 13C APT, COSY NMR, NOESY NMR, 15N NMR, HSQC NMR, HMQC NMR, and HMBC NMR. These are available upon request and may be free or subject to additional charges.
Descrição
Nilotinib EP Impurity B, também designado Nilotinib Related Compound B, corresponde a um aminoálcool aromático de baixa massa molecular, com CAS 18595-18-1, fórmula molecular C9H11NO2 e massa molecular de 165.19 g/mol. A sua estrutura é compatível com um intermediário sintético ou subproduto de processo associado à construção de motivos de benzilamina substituída, e não com uma impureza da classe dos nitrosaminas. A avaliação normalmente exige caracterização ortogonal por LC-MS/MS, MS de alta resolução e RMN, sendo GC-MS útil após derivatização quando a volatilidade o permite. Em contexto regulatório, é controlado como substância relacionada especificada no perfil de impurezas.
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