QNMR, D2O Exchange, 13C NMR, 13C APT, COSY NMR, NOESY NMR, 15N NMR, HSQC NMR, HMQC NMR, and HMBC NMR. These are available upon request and may be free or subject to additional charges.
Descripción
Nilotinib EP Impurity B, designado también Nilotinib Related Compound B, corresponde a un aminoalcohol aromático de bajo peso molecular con CAS 18595-18-1, fórmula molecular C9H11NO2 y peso molecular de 165.19 g/mol. Su estructura es coherente con un intermedio sintético o un subproducto relacionado con el proceso de obtención, vinculado a la formación de motivos de bencilamina sustituida, y no con una impureza de clase nitrosamina. Su evaluación suele requerir caracterización ortogonal mediante LC-MS/MS, MS de alta resolución y RMN, mientras que GC-MS resulta útil tras derivatización cuando la volatilidad lo permite. En el contexto regulatorio se controla como sustancia relacionada especificada dentro del perfil de impurezas.
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