La 6-yodoamilorida (CAS 60398-23-4) es un análogo halogenado de amilorida con fórmula molecular C6H8IN7O y peso molecular de 321,08 g/mol. Como derivado yodado posicional del andamiaje diurético pirazina-guanidinio, suele considerarse una impureza de origen sintético o un análogo relacionado con el proceso, generado por yodación electrofílica o por control incompleto de la sustitución durante la fabricación. Su estructura polar y polibásica, junto con el átomo pesado de yodo, modifica la retención y la ionización respecto de amilorida. Su caracterización y cuantificación a nivel traza requieren habitualmente LC-MS/MS, espectrometría de masas de alta resolución y métodos ortogonales LC-UV, con evaluación de patrones isotópicos y iones de fragmentación.
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