Informações adicionais sobre o 3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate
Impureza 3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate apresenta perfil analítico complexo devido à presença de grupos nitroso | heterociclos aromáticos e o íon piridínio-óxida | conferindo polaridade moderada e forte absorção UV. Recomenda-se caracterização por cromatografia líquida reversa acoplada a espectrometria de massas de alta resolução e RMN para confirmar fórmula e fragmentação. A estabilidade pode ser comprometida em meio redutor ou ácido | com possível redução do nitroso a amina. Para controlo de qualidade e conformidade regulatória recomenda-se validação de métodos quantitativos | investigação de vias de formação e estratégias de purificação para minimizar sua presença no perfil de impurezas.
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![3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate](https://veeprho.com/wp-content/uploads/2024/11/VE0022222-3-2-2-methyl-5-3-4-methyl-1H-imidazol-1-yl-5-trifluoromethyl-phenyl-carbamoyl-phenyl-nitroso-amino-pyrimidin-4-yl-pyridin-1-ium-1-olate-sqr.png "3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate")
![3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate](https://veeprho.com/wp-content/uploads/2026/02/Nilotinib-Hydrochloride-Monohydrate-Working-Standard-Secondary-Reference-Standard-923288-90-8-VE0027614.png "3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate")
![3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate](https://veeprho.com/wp-content/uploads/2022/07/Nilotinib-EP-Impurity-B.png "3-{2-[(2-methyl-5-{[3-(4-methyl-1H-imidazol-1-yl)-5-(trifluoromethyl)phenyl]carbamoyl}phenyl)(nitroso)amino]pyrimidin-4-yl}pyridin-1-ium-1-olate")
