alpha Lipoic Acid Impurity F, CAS 2114407-76-8, es una impureza definida relacionada con el proceso y contiene azufre en el contexto del esqueleto de ácido alfa lipoico. Con fórmula molecular C8H14O3S2 y peso molecular de 222.32 g/mol, corresponde a una especie modificada por oxidación derivada del anillo ditiolano, más que al antioxidante original. Estas impurezas pueden originarse durante la síntesis, en reacciones de intercambio de azufre o por oxidación controlada del sistema disulfuro. Su elucidación suele requerir LC-MS/MS, espectrometría de masas de alta resolución y métodos HPLC ortogonales, mientras que RMN confirma la estructura. Su evaluación se integra en la caracterización de impurezas y el establecimiento de especificaciones bajo principios regulatorios actuales.
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