A impureza associada ao Diclofenac | CAS 15307-79-6 | apresenta características físico-químicas e espectrais específicas que exigem controle rigoroso no perfil de impurezas; caracteriza-se por elevada afinidade lipofílica | solubilidade limitada em água e padrão de absorção UV distinto com máximo em torno de 276 nm. Em cromatografia líquida reversa manifesta tempo de retenção diferenciado em relação ao composto principal e fornece fragmentação característica em espectrometria de massas que facilita identificação e quantificação. A avaliação inclui limites de especificação | estudos de estabilidade forçada e validação analítica para garantir precisão | recuperação e sensibilidade na detecção de impurezas relacionadas.
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